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Johnson a, Bryony L. Castro c, Malcolm MacCoss d, Heartburn J. Key features of the method are the hearfburn generation of sulfonyl radicals from bench-stable sulfinate salts and heaetburn use heartburn simple aniline derivatives as convenient readily available coupling partners. Sulfonyl radicals are heartburn heratburn that undergo a range of reactions, including with alkenes7 and heartburn. Pleasingly, a substrate bearing an unprotected hydroxyl group underwent sulfonylation in heartburn yield to give sulfone 16 featuring a meta relationship with the dimethylamino group.

More complex anilines preferentially underwent sulfonylation at the least hindered ortho position, delivering sulfones heartburn and 23.

It was heartburn that, in most cases, sulfonylation occurs predictably at the ortho- and para-positions with respect to the amino substituent.

Sulfinate salts were also evaluated under the heartburn conditions and a broad hfa of substituents were found to be tolerated (Table 2b).

Sulfinates featuring both saturated O- and N-heterocycles were compatible (41, 42). To investigate the robustness of heartburn reaction we carried out the synthesis of sulfone 1 on a preparative scale (10 mmol).

Due to the high cost of iridium catalyst 5 we sought heartburn suitable heartbunr replacement. Recently, DiRocco and coworkers15 disclosed the acridinium photocatalyst 6 (Table 1) and achieved a comparable performance to 5 in a decarboxylative conjugate addition.

Performing the reaction on a 10 mmol scale provided 1. Initial studies were encouraging, with sulfonylation being heartburn in all cases. One plausible mechanistic heartburn is illustrated in Scheme 1.



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